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Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology

Milić, Petar; Rajković, Katarina; Nikolić, Goran; Jeremić, Sanja; Đurašević, Mirjana

(2023)

TY  - JOUR
AU  - Milić, Petar
AU  - Rajković, Katarina
AU  - Nikolić, Goran
AU  - Jeremić, Sanja
AU  - Đurašević, Mirjana
PY  - 2023
UR  - https://www.sciencedirect.com/science/article/pii/S0263876223000618
UR  - https://imagine.imgge.bg.ac.rs/handle/123456789/1922
AB  - The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu.
T2  - Chemical Engineering Research and Design
T2  - Chemical Engineering Research and DesignChemical Engineering Research and Design
T1  - Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology
EP  - 445
SP  - 439
VL  - 191
DO  - 10.1016/j.cherd.2023.01.051
ER  - 
@article{
author = "Milić, Petar and Rajković, Katarina and Nikolić, Goran and Jeremić, Sanja and Đurašević, Mirjana",
year = "2023",
abstract = "The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu.",
journal = "Chemical Engineering Research and Design, Chemical Engineering Research and DesignChemical Engineering Research and Design",
title = "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology",
pages = "445-439",
volume = "191",
doi = "10.1016/j.cherd.2023.01.051"
}
Milić, P., Rajković, K., Nikolić, G., Jeremić, S.,& Đurašević, M.. (2023). Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design, 191, 439-445.
https://doi.org/10.1016/j.cherd.2023.01.051
Milić P, Rajković K, Nikolić G, Jeremić S, Đurašević M. Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design. 2023;191:439-445.
doi:10.1016/j.cherd.2023.01.051 .
Milić, Petar, Rajković, Katarina, Nikolić, Goran, Jeremić, Sanja, Đurašević, Mirjana, "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology" in Chemical Engineering Research and Design, 191 (2023):439-445,
https://doi.org/10.1016/j.cherd.2023.01.051 . .
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Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology

Milić, Petar; Rajković, Katarina; Nikolić, Goran; Jeremić, Sanja; Đurašević, Mirjana

(2023)

TY  - JOUR
AU  - Milić, Petar
AU  - Rajković, Katarina
AU  - Nikolić, Goran
AU  - Jeremić, Sanja
AU  - Đurašević, Mirjana
PY  - 2023
UR  - https://www.sciencedirect.com/science/article/pii/S0263876223000618
UR  - https://imagine.imgge.bg.ac.rs/handle/123456789/1888
AB  - The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu.
T2  - Chemical Engineering Research and Design
T2  - Chemical Engineering Research and DesignChemical Engineering Research and Design
T1  - Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology
EP  - 445
SP  - 439
VL  - 191
DO  - 10.1016/j.cherd.2023.01.051
ER  - 
@article{
author = "Milić, Petar and Rajković, Katarina and Nikolić, Goran and Jeremić, Sanja and Đurašević, Mirjana",
year = "2023",
abstract = "The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu.",
journal = "Chemical Engineering Research and Design, Chemical Engineering Research and DesignChemical Engineering Research and Design",
title = "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology",
pages = "445-439",
volume = "191",
doi = "10.1016/j.cherd.2023.01.051"
}
Milić, P., Rajković, K., Nikolić, G., Jeremić, S.,& Đurašević, M.. (2023). Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design, 191, 439-445.
https://doi.org/10.1016/j.cherd.2023.01.051
Milić P, Rajković K, Nikolić G, Jeremić S, Đurašević M. Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design. 2023;191:439-445.
doi:10.1016/j.cherd.2023.01.051 .
Milić, Petar, Rajković, Katarina, Nikolić, Goran, Jeremić, Sanja, Đurašević, Mirjana, "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology" in Chemical Engineering Research and Design, 191 (2023):439-445,
https://doi.org/10.1016/j.cherd.2023.01.051 . .
1
1
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Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines

Karabegović, Ivana; Malicanin, Marko; Popović, Nikola; Stamenkovic Stojanović, Sandra; Lazić, Miodrag; Stanojević, Jelena; Danilović, Bojana

(MDPI, Basel, 2022)

TY  - JOUR
AU  - Karabegović, Ivana
AU  - Malicanin, Marko
AU  - Popović, Nikola
AU  - Stamenkovic Stojanović, Sandra
AU  - Lazić, Miodrag
AU  - Stanojević, Jelena
AU  - Danilović, Bojana
PY  - 2022
UR  - https://imagine.imgge.bg.ac.rs/handle/123456789/1585
AB  - The enological potential of two previously characterized indigenous yeast isolates, Hanseniaspora uvarum S-2 and Candida famata WB-1, in pure and sequential inoculation with commercial yeast Saccharomyces cerevisiae QA23 were analyzed in industrial-scale vinification of the grape variety Tamjanika. Their contribution to the quality and aroma profile was investigated by quantifying volatile compounds and wine sensory evaluation. Both yeast isolates were able to complete alcoholic fermentation, to reduce ethanol concentration up to 1.06% v/v (in monoculture) in comparation to S. cerevisiae QA23, and to enhance aroma and sensory profile. Based on calculated odor activity values (OAV), p-cymene, ethyl hexanoate, ethyl octanoate, and ethyl decanoate were the major aroma volatile compounds in all Tamjanika wine samples. Analyzed yeast strains significantly affected relative contribution of volatile compounds and can be considered responsible for the differences and uniqueness of the obtained wine samples. Besides confirmation of good enological and fermentative characteristics, selected isolates can be characterized as high ester-producing strains with potential to enhance the floral and fruity aromas of wine. The present study represents a further step toward the use of indigenous yeast isolates at industrial-scale fermentation in order to ensure the regional signature of Tamjanika wine.
PB  - MDPI, Basel
T2  - Foods
T1  - Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines
IS  - 13
VL  - 11
DO  - 10.3390/foods11131935
ER  - 
@article{
author = "Karabegović, Ivana and Malicanin, Marko and Popović, Nikola and Stamenkovic Stojanović, Sandra and Lazić, Miodrag and Stanojević, Jelena and Danilović, Bojana",
year = "2022",
abstract = "The enological potential of two previously characterized indigenous yeast isolates, Hanseniaspora uvarum S-2 and Candida famata WB-1, in pure and sequential inoculation with commercial yeast Saccharomyces cerevisiae QA23 were analyzed in industrial-scale vinification of the grape variety Tamjanika. Their contribution to the quality and aroma profile was investigated by quantifying volatile compounds and wine sensory evaluation. Both yeast isolates were able to complete alcoholic fermentation, to reduce ethanol concentration up to 1.06% v/v (in monoculture) in comparation to S. cerevisiae QA23, and to enhance aroma and sensory profile. Based on calculated odor activity values (OAV), p-cymene, ethyl hexanoate, ethyl octanoate, and ethyl decanoate were the major aroma volatile compounds in all Tamjanika wine samples. Analyzed yeast strains significantly affected relative contribution of volatile compounds and can be considered responsible for the differences and uniqueness of the obtained wine samples. Besides confirmation of good enological and fermentative characteristics, selected isolates can be characterized as high ester-producing strains with potential to enhance the floral and fruity aromas of wine. The present study represents a further step toward the use of indigenous yeast isolates at industrial-scale fermentation in order to ensure the regional signature of Tamjanika wine.",
publisher = "MDPI, Basel",
journal = "Foods",
title = "Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines",
number = "13",
volume = "11",
doi = "10.3390/foods11131935"
}
Karabegović, I., Malicanin, M., Popović, N., Stamenkovic Stojanović, S., Lazić, M., Stanojević, J.,& Danilović, B.. (2022). Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines. in Foods
MDPI, Basel., 11(13).
https://doi.org/10.3390/foods11131935
Karabegović I, Malicanin M, Popović N, Stamenkovic Stojanović S, Lazić M, Stanojević J, Danilović B. Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines. in Foods. 2022;11(13).
doi:10.3390/foods11131935 .
Karabegović, Ivana, Malicanin, Marko, Popović, Nikola, Stamenkovic Stojanović, Sandra, Lazić, Miodrag, Stanojević, Jelena, Danilović, Bojana, "Native Non-Saccharomyces Yeasts as a Tool to Produce Distinctive and Diverse Tamjanika Grape Wines" in Foods, 11, no. 13 (2022),
https://doi.org/10.3390/foods11131935 . .
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