Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology
Само за регистроване кориснике
2023
Чланак у часопису (Рецензирана верзија)
Метаподаци
Приказ свих података о документуАпстракт
The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yi...eld of micro-elements was Si>Zn>Sr>Cu.
Кључне речи:
Black walnut husk / Minerals / Response surface methodologyИзвор:
Chemical Engineering Research and Design, 2023, 191, 439-445Финансирање / пројекти:
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200017 (Универзитет у Београду, Институт за нуклеарне науке Винча, Београд-Винча) (RS-MESTD-inst-2020-200017)
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200133 (Универзитет у Нишу, Технолошки факултет, Лесковац) (RS-MESTD-inst-2020-200133)
Напомена:
- This is the peer-reviewed version of the article: Milić, P., Rajković, K., Nikolić, G., Jeremić, S.,& Đurašević, M.. (2023). Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design, 191, 439-445. https://doi.org/10.1016/j.cherd.2023.01.051
Повезане информације:
- Друга верзија
https://imagine.imgge.bg.ac.rs/handle/123456789/1888 - Друга верзија
https://doi.org/10.1016/j.cherd.2023.01.051
URI
https://www.sciencedirect.com/science/article/pii/S0263876223000618https://imagine.imgge.bg.ac.rs/handle/123456789/1922
Институција/група
Institut za molekularnu genetiku i genetičko inženjerstvoTY - JOUR AU - Milić, Petar AU - Rajković, Katarina AU - Nikolić, Goran AU - Jeremić, Sanja AU - Đurašević, Mirjana PY - 2023 UR - https://www.sciencedirect.com/science/article/pii/S0263876223000618 UR - https://imagine.imgge.bg.ac.rs/handle/123456789/1922 AB - The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu. T2 - Chemical Engineering Research and Design T2 - Chemical Engineering Research and DesignChemical Engineering Research and Design T1 - Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology EP - 445 SP - 439 VL - 191 DO - 10.1016/j.cherd.2023.01.051 ER -
@article{ author = "Milić, Petar and Rajković, Katarina and Nikolić, Goran and Jeremić, Sanja and Đurašević, Mirjana", year = "2023", abstract = "The aims of this research were preparation of Juglans nigra husk extracts by employing an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. Extracts from J. nigra L. fresh husk were prepared using ethanol (70%, v/v) as a solvent, at different extraction temperatures: 15, 30 and 40 °C, and extraction times: 5, 15, 30, 60 and 80 min. The content of minerals in ethanol extracts was determined using inductively coupled plasma optical emission spectrometry (ICP-OES). The response surface methodology (RSM) was developed to evaluate the effect of two extraction factors as well as to optimize the extraction variables for each mineral individually. The RSM models pointed out 40 °C temperature and extraction time in the range 77–80 min as optimal conditions for extraction of macro- and micro-elements. Results of RSM optimization showed the relative order of maximum obtained yield of macro-elements: K>P>S>Ca>Mg and maximum yield of micro-elements was Si>Zn>Sr>Cu.", journal = "Chemical Engineering Research and Design, Chemical Engineering Research and DesignChemical Engineering Research and Design", title = "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology", pages = "445-439", volume = "191", doi = "10.1016/j.cherd.2023.01.051" }
Milić, P., Rajković, K., Nikolić, G., Jeremić, S.,& Đurašević, M.. (2023). Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design, 191, 439-445. https://doi.org/10.1016/j.cherd.2023.01.051
Milić P, Rajković K, Nikolić G, Jeremić S, Đurašević M. Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology. in Chemical Engineering Research and Design. 2023;191:439-445. doi:10.1016/j.cherd.2023.01.051 .
Milić, Petar, Rajković, Katarina, Nikolić, Goran, Jeremić, Sanja, Đurašević, Mirjana, "Preparation of Juglans nigra L. husk extracts by applying an ultrasonic-assisted extraction method and process optimization of minerals extraction using response surface methodology" in Chemical Engineering Research and Design, 191 (2023):439-445, https://doi.org/10.1016/j.cherd.2023.01.051 . .